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Antrim, BT2 8FD, United Kingdom"}],"cl_hierarchyLevel":[{"key":"dataset","default":"Dataset","langeng":"Dataset","link":"http://standards.iso.org/iso/19139/resources/gmxCodelists.xml#MD_ScopeCode"}],"cl_maintenanceAndUpdateFrequency":[{"key":"notPlanned","default":"Not planned","langeng":"Not planned","link":"http://standards.iso.org/iso/19139/resources/gmxCodelists.xml#MD_MaintenanceFrequencyCode"}],"cl_type":[{"key":"theme","default":"Theme","langeng":"Theme","link":"http://standards.iso.org/iso/19139/resources/gmxCodelists.xml#MD_KeywordTypeCode"}],"cl_accessConstraints":[{"key":"otherRestrictions","default":"Other restrictions","langeng":"Other restrictions","link":"http://standards.iso.org/iso/19139/resources/gmxCodelists.xml#MD_RestrictionCode"}],"cl_spatialRepresentationType":[{"key":"vector","default":"Vector","langeng":"Vector","link":"http://standards.iso.org/iso/19139/resources/gmxCodelists.xml#MD_SpatialRepresentationTypeCode"}],"resourceTitleObject":{"default":"The Tellus Urban Soil Survey of Northern Ireland","langeng":"The Tellus Urban Soil Survey of Northern Ireland"},"creationDateForResource":["2007-01-01T00:00:00.000Z"],"creationYearForResource":"2007","creationMonthForResource":"2007-01","resourceDate":[{"type":"creation","date":"2007-01-01T00:00:00.000Z"}],"resourceTemporalDateRange":[{"gte":"2007-01-01T00:00:00.000Z","lte":"2007-01-01T00:00:00.000Z"},{"gte":"2005-01-01T00:00:00.000Z","lte":"2006-12-31T00:00:00.000Z"}],"resourceIdentifier":[{"code":"https://gsni-data.bgs.ac.uk/geonetwork/srv/api/records/174dbca4-a3e7-4bbb-91b9-f7919b6e2a44","codeSpace":"","link":""}],"resourceAbstractObject":{"default":"The Geological Survey of Northern Ireland (GSNI) and the British Geological Survey (BGS) completed a regional geochemical survey of Northern Ireland's soils, sediments and waters between 2004 and 2006.\n\nSoil sampling of all of Northern Ireland was completed under the Tellus survey between 2004 and 2006. Soil samples were collected on a systematic basis from rural areas in most of the region, excluding only the major urban centres of Belfast and Bangor. Soils were also collected at a higher sampling density from the urban areas of Belfast, Bangor, Carrickfergus, Carryduff, Castlereagh, Greenisland, Holywood, Lisburn, Newtownabbey and Londonderry, although these urban results are not reported here.\n\nIn rural areas, samples were collected from alternate 1 km Irish national- grid squares. Site selection within each square was random, subject to the avoidance wherever possible of roads, tracks, railways, human habitation and other disturbed ground. At each site two composite samples of five auger flights were collected, each composite sample comprising approximately 750 g of unsieved material. Samples were collected using a hand auger with a 20 by 5 cm flight from a standard depth interval of 5–20 cm for designated ‘A’ samples, referred to subsequently as ‘surface soils’, and at 35–50 cm for designated ‘S’ samples (nominally the B horizon), referred to subsequently as ‘deep soils’. Some 6,862 regional soil sites were sampled (see supplementary map - soil locations) and analysed, resulting in an average regional sampling density of 1 site per 2 km2. Observations of soil colour, depth, clast lithology and abundance were recorded at site. The samples were classified into five textural groups (sand, sand-silt, silt, silt-clay and clay).\n\nThe methods used for urban soils were similar except that (1) the sample density was higher, at four sites per square kilometre; (2) the sample sites corresponded closely to a predefined grid and did not avoid areas of human influence. In addition, extra samples requiring special treatment were taken for the determination of selected organic constituents (Smyth, 2009: especially Appendix 1).\n\nAt each soil sample site, information on the location, site and catchment geology, contamination, land use, and other features required for data interpretation were entered onto field cards. The sample location was also plotted on a field copy of the 1:50 000 Ordnance Survey of Northern Ireland (OSNI) map.\n\nObservations from field cards were entered into a digital Access2000™ database after undergoing a field quality control process (Lister et al, 2005). This involved checking that the correct codes had been recorded on field cards and that GPS coordinates recorded on the card matched those in the GPS unit for each site. Thus both a traditional paper archive of observations was maintained as well as the construction of a computerised database.\n\nSoils were initially air-dried at the field-base prior to transport to the sample store where they were dried in a temperature controlled oven at 30°C for 2–3 days. At the end of each field campaign samples were checked against field sheets prior to packing for transport to the BGS laboratory for sample preparation. On arrival at the laboratory samples were checked against shipping lists prior to assigning laboratory batch numbers in the BGS UKAS Quality Assurance System. The A and S soils were prepared in the same manner in a trace-level sample preparation laboratory.\n\nSamples were disaggregated prior to sieving to a <2 mm fraction using nylon mesh. Replicate samples were prepared by riffle splitting each of the duplicate samples. Soil pH and LOI was determined for every A surface soil sample. A representative 30 g (± 2 g) sub-sample was obtained by cone and quartering. This sub-sample was then milled in an agate ball mill at 300 rpm for 30 minutes.\n\nDifferent analytical procedures were employed for the surface and deep soils. Pressed pellet production and XRF analysis were completed by laboratory on surface soils only. Sub-samples of milled soil were weighed and placed into tamper-evident plastic sample tubes. The XRF pressed pellet was prepared by adding an aliquot (3 g ±0.05 g) of two blended synthetic waxes comprising 90 % EMU 120 FD wax and 10 % Ceridust (both waxes are styrene based co-polymers) to 12 g (± 0.05 g) of milled material. This mixture was milled for 4 minutes at 300 rpm. On completion of the binder milling the prepared powders were placed into tamper evident plastic sample tubes for temporary storage prior to pellet preparation. Pellets (40 mm) were pressed using a calibrated Herzog semi-automatic pellet press at 25 kN.\n\nPrior to analysis, concealed certified reference materials and secondary reference materials were inserted into the sample batches. XRF analysis of the A samples was undertaken at the BGS; ICP analysis of A and S samples at SGS Laboratories, Toronto; and fire-assay of S samples at SGS Laboratories, Toronto.\n\nFor the Tellus samples, Energy Dispersive Polarised X-Ray Fluorescence (ED(P)- XRF) spectrometers were used to analyse those elements for which the WD-XRF spectrometers were insufficiently sensitive. Certified Reference Material (CRM) standards were used to calibrate the instruments. The PANalytical software was used for spectral deconvolution and to fit calibration curves, applying matrix correction by internal ratio Compton correction method. The calibrations were validated by analysis of a wide range of RMs. The detectors were calibrated weekly. All backgrounds and peaks were corrected for instrument drift using two external ratio monitors, when required. Quality control was maintained by regular analysis of two glass monitor samples containing 47 elements at nominally 30 mg/ kg and 300 mg/kg. Results were presented as run charts for statistical analysis using statistical process control software (SPC).\n\nThe lower limits of detection are theoretical values for the concentration equivalent to three standard deviations (99.7 % confidence interval) above the background count rate for the analyte in an iron-rich alumino-silicate matrix. For silicate matrices the practical detection limits for most elements approach the theoretical values due to high instrumental stability. LLDs were calculated from a matrix blank and the ‘synthetic’ Pro-Trace standards.\n\nIndividual results are not reliable below the quoted lower limits, but reliable estimates of the average or typical values over an area may be obtained at lower levels of concentration; meaningful distribution patterns may thus be recognised for some elements at levels lower than the LLD.\n\nThe data are described in Young, Mike; Donald, Alex, eds. 2013 A guide to the Tellus data. Belfast, UK, Geological Survey of Northern Ireland, 233pp. available for free download from: http://nora.nerc.ac.uk/509171/\n\nThe Tellus survey was funded by the Department of Enterprise, Trade and Investment (DETI), now the Department for the Economy (DfE) in Northern Ireland and the INTERREG IVA programme of the European Union (EU) Regional Development Fund.","langeng":"The Geological Survey of Northern Ireland (GSNI) and the British Geological Survey (BGS) completed a regional geochemical survey of Northern Ireland's soils, sediments and waters between 2004 and 2006.\n\nSoil sampling of all of Northern Ireland was completed under the Tellus survey between 2004 and 2006. Soil samples were collected on a systematic basis from rural areas in most of the region, excluding only the major urban centres of Belfast and Bangor. Soils were also collected at a higher sampling density from the urban areas of Belfast, Bangor, Carrickfergus, Carryduff, Castlereagh, Greenisland, Holywood, Lisburn, Newtownabbey and Londonderry, although these urban results are not reported here.\n\nIn rural areas, samples were collected from alternate 1 km Irish national- grid squares. Site selection within each square was random, subject to the avoidance wherever possible of roads, tracks, railways, human habitation and other disturbed ground. At each site two composite samples of five auger flights were collected, each composite sample comprising approximately 750 g of unsieved material. Samples were collected using a hand auger with a 20 by 5 cm flight from a standard depth interval of 5–20 cm for designated ‘A’ samples, referred to subsequently as ‘surface soils’, and at 35–50 cm for designated ‘S’ samples (nominally the B horizon), referred to subsequently as ‘deep soils’. Some 6,862 regional soil sites were sampled (see supplementary map - soil locations) and analysed, resulting in an average regional sampling density of 1 site per 2 km2. Observations of soil colour, depth, clast lithology and abundance were recorded at site. The samples were classified into five textural groups (sand, sand-silt, silt, silt-clay and clay).\n\nThe methods used for urban soils were similar except that (1) the sample density was higher, at four sites per square kilometre; (2) the sample sites corresponded closely to a predefined grid and did not avoid areas of human influence. In addition, extra samples requiring special treatment were taken for the determination of selected organic constituents (Smyth, 2009: especially Appendix 1).\n\nAt each soil sample site, information on the location, site and catchment geology, contamination, land use, and other features required for data interpretation were entered onto field cards. The sample location was also plotted on a field copy of the 1:50 000 Ordnance Survey of Northern Ireland (OSNI) map.\n\nObservations from field cards were entered into a digital Access2000™ database after undergoing a field quality control process (Lister et al, 2005). This involved checking that the correct codes had been recorded on field cards and that GPS coordinates recorded on the card matched those in the GPS unit for each site. Thus both a traditional paper archive of observations was maintained as well as the construction of a computerised database.\n\nSoils were initially air-dried at the field-base prior to transport to the sample store where they were dried in a temperature controlled oven at 30°C for 2–3 days. At the end of each field campaign samples were checked against field sheets prior to packing for transport to the BGS laboratory for sample preparation. On arrival at the laboratory samples were checked against shipping lists prior to assigning laboratory batch numbers in the BGS UKAS Quality Assurance System. The A and S soils were prepared in the same manner in a trace-level sample preparation laboratory.\n\nSamples were disaggregated prior to sieving to a <2 mm fraction using nylon mesh. Replicate samples were prepared by riffle splitting each of the duplicate samples. Soil pH and LOI was determined for every A surface soil sample. A representative 30 g (± 2 g) sub-sample was obtained by cone and quartering. This sub-sample was then milled in an agate ball mill at 300 rpm for 30 minutes.\n\nDifferent analytical procedures were employed for the surface and deep soils. Pressed pellet production and XRF analysis were completed by laboratory on surface soils only. Sub-samples of milled soil were weighed and placed into tamper-evident plastic sample tubes. The XRF pressed pellet was prepared by adding an aliquot (3 g ±0.05 g) of two blended synthetic waxes comprising 90 % EMU 120 FD wax and 10 % Ceridust (both waxes are styrene based co-polymers) to 12 g (± 0.05 g) of milled material. This mixture was milled for 4 minutes at 300 rpm. On completion of the binder milling the prepared powders were placed into tamper evident plastic sample tubes for temporary storage prior to pellet preparation. Pellets (40 mm) were pressed using a calibrated Herzog semi-automatic pellet press at 25 kN.\n\nPrior to analysis, concealed certified reference materials and secondary reference materials were inserted into the sample batches. XRF analysis of the A samples was undertaken at the BGS; ICP analysis of A and S samples at SGS Laboratories, Toronto; and fire-assay of S samples at SGS Laboratories, Toronto.\n\nFor the Tellus samples, Energy Dispersive Polarised X-Ray Fluorescence (ED(P)- XRF) spectrometers were used to analyse those elements for which the WD-XRF spectrometers were insufficiently sensitive. Certified Reference Material (CRM) standards were used to calibrate the instruments. The PANalytical software was used for spectral deconvolution and to fit calibration curves, applying matrix correction by internal ratio Compton correction method. The calibrations were validated by analysis of a wide range of RMs. The detectors were calibrated weekly. All backgrounds and peaks were corrected for instrument drift using two external ratio monitors, when required. Quality control was maintained by regular analysis of two glass monitor samples containing 47 elements at nominally 30 mg/ kg and 300 mg/kg. Results were presented as run charts for statistical analysis using statistical process control software (SPC).\n\nThe lower limits of detection are theoretical values for the concentration equivalent to three standard deviations (99.7 % confidence interval) above the background count rate for the analyte in an iron-rich alumino-silicate matrix. For silicate matrices the practical detection limits for most elements approach the theoretical values due to high instrumental stability. LLDs were calculated from a matrix blank and the ‘synthetic’ Pro-Trace standards.\n\nIndividual results are not reliable below the quoted lower limits, but reliable estimates of the average or typical values over an area may be obtained at lower levels of concentration; meaningful distribution patterns may thus be recognised for some elements at levels lower than the LLD.\n\nThe data are described in Young, Mike; Donald, Alex, eds. 2013 A guide to the Tellus data. 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A total of 114 samples were collected. Samples were collected randomly from outcrops across Northern Ireland.\n\nSeveral donated samples of mineralisation from Curraghinalt (gold bearing base metals), South Armagh (base-metal) and Whitespots (lead mineralisation) were incorporated into the lithogeochemical program. In all cases only fresh unaltered material was collected/ analysed. At each site a c.15 kg representative sample of each outcrop was collected. Samples were prepared at the laboratories of the British Geological Survey, Keyworth, Nottingham. Preparation consisted of an initial thorough washing of the sample to remove any rock or soil debris. Samples were then chipped and 100 g of material was milled in an agate ball-mill to a specification identical to that for the soils. The rock powders were dried overnight at 105°C before loss on ignition (L.O.I.) and fused bead production. Any samples with visible mineralisation were prepared in a similar manner but in a separate facility dedicated to higher grade materials. The fused bead XRFS analysis was completed at the laboratories of the British Geological Survey.\n\nAll other analytical tests were completed at SGS Laboratories (Toronto). The analytical methods and detection limits for the lithogeochemical trace element suite are presented in Table 2 in the report https://nora.nerc.ac.uk/id/eprint/14008/1/OR07022.pdf. The parameters of lithogeochemical analyses were as follows;\n\n1. Fused bead XRF- for major oxides.\n2. Loss of ignition- determined after 1 hour at 1050°C.\n3. Au, Pd, Pt Fire Assay/ ICP-MS- a 30 g sample was analysed. SGS Laboratories method code FAM303.\n4. Multi-element suite by sodium peroxide fusion- completed on a 0.5 g sample with analysis by ICP-MS. SGS Laboratories method code ICM90A.\n5. F by Specific Ion- completed on a 0.5 g sample. SGS Laboratories method code ISE07A.\n6. C by Leco- completed on a 0.5 g sample. SGS Laboratories method code CSA01V.\n7. S by Leco- completed on a 0.5 g sample. SGS Laboratories method code CSA06V.\n8. Hg by Cold-Vapour Atomic Absorption Spectrometry- completed on a 0.6 g sample. SGS Laboratories method code CVA14C.\n\nPrior to analysis certified reference materials and secondary reference materials were inserted into the sample batches. All reference materials were concealed in the sample batches sent for analysis. Chinese lithogeochemical certified reference materials GSR-1 to GSR-6 were used for all analytical tests (China National Analysis Center for Iron and Steel, 1986), except Au, Pd and Pt by fire assay.\n\nThe parameters of the GSR-1 to 6 reference materials are as follows;\n\nGSR-1 Grey medium-grained biotite granite sample from Qianlishan rock body in Chenzhou, Hunan. Also referred to as GBW07103.\nGSR-2 Mesozoic quartz hornblende andesite from the vicinity of the Meishan iron mine in Nanjing, Jiangsu. Also referred to as GBW07104.\nGSR-3 Cenozoic alkali-olivine basalt from Zhangjiakou, Hebei. Also referred to as GBW07105.\nGSR-4 Light and dark arkosic quartz-sandstone from Group Wutong, Silurian system in Tongling, Anhui. Also referred to as GBW07106.\nGSR-5 Shale from Group Chuanlinggou, Sinian system in Jixian, Tianjin. Also referred to as GBW07107.\nGSR-6 Banded argillaceous limestone, Triassic system in Tongling, Anhui. Also referred to as GBW07108.\n\nFor the analysis of Au, Pd, and Pt by fire assay the following CANMET Reference Materials (RMs) were used; TDB-1, WPR-1, and WGB-1. Separate insertions of the CANMET RM’s were also analysed and reported by SGS as part of the fire assay analysis. All GSR series and CANMET RMs were inserted into their respective batches at a rate of three samples per 87 field samples. Four field duplicate pairs were collected per field batch (100 samples). Secondary reference soils Antbas, Dal, LwrPala and S13B were inserted in rotation at a rate of two samples per field batch. Due to the unavailability of lithogeochemical secondary reference materials it was not possible to matrix match SRMs to the survey.\n\nAll analyses at SGS Laboratories were completed by a combination of ICP-OES and ICP-MS instrumentation. Data were reported as censored and uncensored datasets.\n\nThe Tellus survey was funded by the Department of Enterprise, Trade and Investment (DETI), now the Department for the Economy (DfE) in Northern Ireland and the INTERREG IVA programme of the European Union (EU) Regional Development Fund.","langeng":"A reconnaissance rock sampling programme was completed after the main phase of Tellus fieldwork. A total of 114 samples were collected. Samples were collected randomly from outcrops across Northern Ireland.\n\nSeveral donated samples of mineralisation from Curraghinalt (gold bearing base metals), South Armagh (base-metal) and Whitespots (lead mineralisation) were incorporated into the lithogeochemical program. In all cases only fresh unaltered material was collected/ analysed. At each site a c.15 kg representative sample of each outcrop was collected. Samples were prepared at the laboratories of the British Geological Survey, Keyworth, Nottingham. Preparation consisted of an initial thorough washing of the sample to remove any rock or soil debris. Samples were then chipped and 100 g of material was milled in an agate ball-mill to a specification identical to that for the soils. The rock powders were dried overnight at 105°C before loss on ignition (L.O.I.) and fused bead production. Any samples with visible mineralisation were prepared in a similar manner but in a separate facility dedicated to higher grade materials. The fused bead XRFS analysis was completed at the laboratories of the British Geological Survey.\n\nAll other analytical tests were completed at SGS Laboratories (Toronto). The analytical methods and detection limits for the lithogeochemical trace element suite are presented in Table 2 in the report https://nora.nerc.ac.uk/id/eprint/14008/1/OR07022.pdf. The parameters of lithogeochemical analyses were as follows;\n\n1. Fused bead XRF- for major oxides.\n2. Loss of ignition- determined after 1 hour at 1050°C.\n3. Au, Pd, Pt Fire Assay/ ICP-MS- a 30 g sample was analysed. SGS Laboratories method code FAM303.\n4. Multi-element suite by sodium peroxide fusion- completed on a 0.5 g sample with analysis by ICP-MS. SGS Laboratories method code ICM90A.\n5. F by Specific Ion- completed on a 0.5 g sample. SGS Laboratories method code ISE07A.\n6. C by Leco- completed on a 0.5 g sample. SGS Laboratories method code CSA01V.\n7. S by Leco- completed on a 0.5 g sample. SGS Laboratories method code CSA06V.\n8. Hg by Cold-Vapour Atomic Absorption Spectrometry- completed on a 0.6 g sample. SGS Laboratories method code CVA14C.\n\nPrior to analysis certified reference materials and secondary reference materials were inserted into the sample batches. All reference materials were concealed in the sample batches sent for analysis. Chinese lithogeochemical certified reference materials GSR-1 to GSR-6 were used for all analytical tests (China National Analysis Center for Iron and Steel, 1986), except Au, Pd and Pt by fire assay.\n\nThe parameters of the GSR-1 to 6 reference materials are as follows;\n\nGSR-1 Grey medium-grained biotite granite sample from Qianlishan rock body in Chenzhou, Hunan. Also referred to as GBW07103.\nGSR-2 Mesozoic quartz hornblende andesite from the vicinity of the Meishan iron mine in Nanjing, Jiangsu. Also referred to as GBW07104.\nGSR-3 Cenozoic alkali-olivine basalt from Zhangjiakou, Hebei. Also referred to as GBW07105.\nGSR-4 Light and dark arkosic quartz-sandstone from Group Wutong, Silurian system in Tongling, Anhui. Also referred to as GBW07106.\nGSR-5 Shale from Group Chuanlinggou, Sinian system in Jixian, Tianjin. Also referred to as GBW07107.\nGSR-6 Banded argillaceous limestone, Triassic system in Tongling, Anhui. Also referred to as GBW07108.\n\nFor the analysis of Au, Pd, and Pt by fire assay the following CANMET Reference Materials (RMs) were used; TDB-1, WPR-1, and WGB-1. Separate insertions of the CANMET RM’s were also analysed and reported by SGS as part of the fire assay analysis. All GSR series and CANMET RMs were inserted into their respective batches at a rate of three samples per 87 field samples. Four field duplicate pairs were collected per field batch (100 samples). Secondary reference soils Antbas, Dal, LwrPala and S13B were inserted in rotation at a rate of two samples per field batch. 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to the Tellus Data edited by Young, M.E. and Donald, A.W. can be downloaded at https://nora.nerc.ac.uk/id/eprint/509171/\n\nMethods used in the Tellus Geochemical Mapping of Northern Ireland Tellus Geochemistry Programme Open Report OR/07/022 https://nora.nerc.ac.uk/id/eprint/14008/1/OR07022.pdf\n\nA reconnaissance rock sampling programme was completed after the main phase of Tellus fieldwork. 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Stream sampling over eastern counties was undertaken by the GSNI and the BGS under the Tellus survey in 2005 and 2006.\n\n2908 stream sediment samples were collected during the summers of 1994 to 1996 by the BGS and a further 2966 in 2005/6 by the Tellus survey. Where possible, sites were situated on first or second-order streams. The combined surveys produced an average sampling density of one site per 2.4 km².\n\nAs far as possible, samples were collected from active sediment, upstream of any potential source of contamination, such as habitation, industrial activity or any road or track crossing. Samples were collected by pairs of samplers, usually university students. The sampling and data recording procedures were standardised before the main survey. Sampling teams were changed daily to reduce the possibility of sampling bias.\n\nThe sediment sample was collected after removal of the oxidised surface material and was wet-screened on site using a method devised by B A Toms (Department of Chemistry, University of Birmingham). This method uses a minimum of water to collect the fraction of sediment finer than 150 µm. Approximately 100 g of material was collected in a Kraft™ paper bag. A heavy-mineral concentrate was obtained at each site by screening the stream sediment through a 2 mm sieve and panning 2–3 kg of this sieved material using the method described by Leake and Aucott (1973).\n\nIn the 1994/6 survey, stream sediment samples were freeze-dried and then ground to <50 µm at a field laboratory. During the Tellus field campaign, 2005/6, samples were air-dried prior to dispatch in batches of 100 to an interim storage facility. Further air-drying was completed at the store to a level that would allow samples to be packaged for onward transport to the BGS analytical laboratory. On arrival at the laboratory samples were checked against shipping lists prior to assigning laboratory batch numbers in the BGS UKAS Quality Assurance System. If necessary, the dried Tellus sediment samples were disaggregated by hand in a mortar and pestle. Tellus sediment samples were freeze-dried under reduced pressure within a pre-set temperature range of -30°C to 30°C for a minimum of 24 hours. Transposition of sample numbers and cross contamination of samples were prevented by preparing each sample individually.\n\nThe data are described in Young, Mike; Donald, Alex, eds. 2013 A guide to the Tellus data. Belfast, UK, Geological Survey of Northern Ireland, 233pp. available for free download from: http://nora.nerc.ac.uk/509171/\n\nStream Sediments Fire Assay\nStream sediment and S soils were analysed by fire assay for gold, palladium and platinum. The 1994/6 stream sediment samples were analysed in early 2002 at Acme Analytical Laboratories Ltd. (Vancouver), who also analysed the Tellus stream sediments. SGS Laboratories analysed the Tellus S soils. For both sample types 10 g sub-samples of milled material were prepared and dispatched to the analytical contractors by the BGS laboratory. A standard lead fire assay process was completed on samples in both laboratories. Soil samples were fired for 60 minutes with a flux mixture containing lead oxide (litharge) in a gas furnace at 1050ºC ±100ºC. Sediment samples were fired for 40 minutes. Silver was added in order to alloy the precious metals and produce a bead at the end of the cupellation process. On completion of the firing the resulting lead button was separated from the borosilicate slag and subsequently heated in a MnO cupel for 1 hour. This removed the lead and produced a silver bead containing Au, Pt and Pd (and Rh).\n\nFor the soil analysis the bead was digested in 0.5 mL of 1:1 nitric acid and 0.5 mL of hydrochloric acid and then diluted to 5 mL with water. For sediments the bead was digested with 1 mL of hot nitric acid (HNO3) and then 10 mL of hydrochloric acid (HCl). In both laboratories a portion of the digested silver bead was aspirated into the Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) where the concentrations of Au, Pd and Pt were determined against calibration standards. A semi-quantitative analysis of rhodium was obtained in stream sediment samples. Soil samples were analysed on a Perkin Elmer Sciex Elan 9000 ICP-MS Spectrometer and sediment samples on a Perkin Elmer Elan 6000 ICP-MS Spectrometer. Quoted detection limits for soil and sediment analysis are shown in Table 3. For soils the calibration curve consisted of four points: blank, 10, 25 and 50 µg/L for each of gold, palladium and platinum in solution. An independent check solution at 10 µg/mL was analysed after the calibration, a ±10 % tolerance had to be met before analysis commenced.\n\nStream Sediments: Boron analysis by ICP-MS\nBoron analyses of stream sediments, contemporaneous with the fire assay, were performed at Acme Analytical Laboratories Ltd. (Vancouver) as this element cannot be determined by XRF. A 0.10 g sub-sample of milled sediment was weighed into a zirconium crucible and mixed with 1.5 g Na2O2 and 0.5 g NaOH. Analysis was completed by ICP-MS using a single spectrometer (ICP13) in the case of Tellus samples. The quoted detection limit was 2 mg/kg. Internal laboratory quality control was completed in accordance with the procedures outlined for the Acme Laboratories fire assay analysis. Quality control of 1994/6 samples was monitored using internal standard LIB-10. For Tellus samples quality control was monitored using internal standards C3, FA-100S and LIBF200\n\nThe Tellus survey was funded by the Department of Enterprise, Trade and Investment (DETI), now the Department for the Economy (DfE) in Northern Ireland and the INTERREG IVA programme of the European Union (EU) Regional Development Fund.","langeng":"Stream sediment from western Northern Ireland were collected by British Geological Survey (BGS) between 1994 and 1996. Stream sampling over eastern counties was undertaken by the GSNI and the BGS under the Tellus survey in 2005 and 2006.\n\n2908 stream sediment samples were collected during the summers of 1994 to 1996 by the BGS and a further 2966 in 2005/6 by the Tellus survey. Where possible, sites were situated on first or second-order streams. The combined surveys produced an average sampling density of one site per 2.4 km².\n\nAs far as possible, samples were collected from active sediment, upstream of any potential source of contamination, such as habitation, industrial activity or any road or track crossing. Samples were collected by pairs of samplers, usually university students. The sampling and data recording procedures were standardised before the main survey. Sampling teams were changed daily to reduce the possibility of sampling bias.\n\nThe sediment sample was collected after removal of the oxidised surface material and was wet-screened on site using a method devised by B A Toms (Department of Chemistry, University of Birmingham). This method uses a minimum of water to collect the fraction of sediment finer than 150 µm. Approximately 100 g of material was collected in a Kraft™ paper bag. 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In both laboratories a portion of the digested silver bead was aspirated into the Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) where the concentrations of Au, Pd and Pt were determined against calibration standards. A semi-quantitative analysis of rhodium was obtained in stream sediment samples. Soil samples were analysed on a Perkin Elmer Sciex Elan 9000 ICP-MS Spectrometer and sediment samples on a Perkin Elmer Elan 6000 ICP-MS Spectrometer. Quoted detection limits for soil and sediment analysis are shown in Table 3. For soils the calibration curve consisted of four points: blank, 10, 25 and 50 µg/L for each of gold, palladium and platinum in solution. An independent check solution at 10 µg/mL was analysed after the calibration, a ±10 % tolerance had to be met before analysis commenced.\n\nStream Sediments: Boron analysis by ICP-MS\nBoron analyses of stream sediments, contemporaneous with the fire assay, were performed at Acme Analytical Laboratories Ltd. 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